1-N-acetyl-4-benzyloxypiperidine

Base Information

Chemical Name:1-N-acetyl-4-benzyloxypiperidine
CAS No.:440122-22-5
Molecular Formula:C₁₄H₁₉NO₂
Molecular Weight:233.31
Hs Code.:

Synonyms:1-N-acetyl-4-benzyloxypiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-N-acetyl-4-benzyloxypiperidine

Chemical Property:

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Technology Process of 1-N-acetyl-4-benzyloxypiperidine

There total 1 articles about 1-N-acetyl-4-benzyloxypiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 32161-06-1
1-acetyl-4-piperidinone

: 100-39-0
benzyl bromide

: 440122-22-5
1-N-acetyl-4-benzyloxypiperidine

Guidance literature:: 1-acetyl-4-piperidinone; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Further stages.;
DOI:10.1039/b110428b

Reference yield: 55.0%

: 440122-22-5
1-N-acetyl-4-benzyloxypiperidine

: 440122-05-4
1-N-acetyl-4-(α-azidobenzyloxy)piperidine

Guidance literature:: With sodium azide; Iodine monochloride; In acetonitrile; at 80 ℃; for 0.666667h;
DOI:10.1039/b110428b

Reference yield:

: 440122-22-5
1-N-acetyl-4-benzyloxypiperidine

: 1-N-acetyl-4-(α-methylbenzyloxy)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / ICl; NaN₃ / acetonitrile / 0.67 h / 80 °C

2: 94 percent / toluene; diethyl ether / 0.17 h / 25 °C

With sodium azide; Iodine monochloride; In diethyl ether; toluene; acetonitrile;
DOI:10.1039/b110428b