benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

Base Information

Chemical Name:benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate
CAS No.:1443792-99-1
Molecular Formula:C₇H₈O₃S*C₂₂H₂₁NO₃
Molecular Weight:519.618
Hs Code.:

Synonyms:benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

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Chemical Property of benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

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Technology Process of benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

There total 1 articles about benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104-15-4
toluene-4-sulfonic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 336877-72-6
L-2-[p-(benzyloxy)phenyl]glycine

: 1443792-99-1
benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

Guidance literature:: In benzene; for 12h; Reflux;
DOI:10.1021/jo4007893

Reference yield: 76.0%

: 3262-72-4
(S)-N-(tert-butoxycarbonyl)serine

: 1443792-99-1
benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

: 1443793-00-7
N-tert-butyloxycarbonyl-L-serine-L-[p-(benzyloxy)phenyl]glycine benzyl ester

Guidance literature:: (S)-N-(tert-butoxycarbonyl)serine; With (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 ℃; for 0.0166667h;

benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;
DOI:10.1021/jo4007893

Reference yield:

: 1443792-99-1
benzyl-L-[p-(benzyloxy)phenyl]glycine toluenesulfonate

: 1443793-02-9
N-tert-butyloxycarbonyl-D-[p-(benzyloxy)phenyl]glycine-L-serine-L-[p-(benzyloxy)phenyl]glycine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / dichloromethane; N,N-dimethyl-formamide / 0.02 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.02 h / 0 °C

3.2: 3 h / 0 - 20 °C

With (benzotriazol-1-yloxy)tripyrrolodinophosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo4007893