C₂₃H₃₀ClN₅O

Base Information

Chemical Name:C₂₃H₃₀ClN₅O
CAS No.:1005143-10-1
Molecular Formula:C₂₃H₃₀ClN₅O
Molecular Weight:427.977
Hs Code.:

C<sub>23</sub>H<sub>30</sub>ClN<sub>5</sub>O

Synonyms:C₂₃H₃₀ClN₅O

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Chemical Property of C₂₃H₃₀ClN₅O

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Technology Process of C₂₃H₃₀ClN₅O

There total 7 articles about C₂₃H₃₀ClN₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960292-46-0
6-benzyl-3-chloro-2-methyl-5-(2-methyl-propanoyl)-6H-pyrazolo[1,5-c]pyrimidin-7-one

: 109-55-7
1-amino-3-(dimethylamino)propane

: 1005143-10-1
C₂₃H₃₀ClN₅O

Guidance literature:: With titanium(IV) isopropylate; at 50 ℃; for 16h;

Reference yield:

: 960292-68-6
6-benzyl-3-chloro-2-methyl-7-oxo-6,7-dihydro-pyrazolo[1,5-c]pyrimidine-5-carbaldehyde

: 1005143-10-1
C₂₃H₃₀ClN₅O

Guidance literature:: Multi-step reaction with 3 steps

1.1: methyllithium / tetrahydrofuran; diethyl ether / 1 h / -78 °C

1.2: 2 h

2.1: 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.2: 16 h / 20 °C

3.1: titanium(IV) isopropylate / 16 h / 50 °C

With titanium(IV) isopropylate; methyllithium; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 1004-36-0
2,6-dimethylpyrone

: 1005143-10-1
C₂₃H₃₀ClN₅O

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide; ethanol; water / 6 h / 60 - 100 °C

2.1: sodium carbonate / water / 1 h / 100 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C

4.1: N-chloro-succinimide / tetrachloromethane / 5 h / Heating / reflux

5.1: selenium(IV) oxide / 1,4-dioxane / 5 h / Heating / reflux

6.1: methyllithium / tetrahydrofuran; diethyl ether / 1 h / -78 °C

6.2: 2 h

7.1: 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve

7.2: 16 h / 20 °C

8.1: titanium(IV) isopropylate / 16 h / 50 °C

With titanium(IV) isopropylate; selenium(IV) oxide; sodium hydroxide; N-chloro-succinimide; ethanol; water; methyllithium; sodium carbonate; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;