(2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

Base Information

Chemical Name:(2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol
CAS No.:204127-03-7
Molecular Formula:C₂₁H₂₅NO₄
Molecular Weight:355.434
Hs Code.:

Synonyms:(2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

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Chemical Property of (2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

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Technology Process of (2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

There total 3 articles about (2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 192764-07-1
N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenyl-methyl]-hydroxylamine

: 204127-03-7
(2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

Guidance literature:: With pyridine; In dichloromethane; Ambient temperature;
DOI:10.1021/jo971913n

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 204127-03-7
(2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₂AlCl / 1.) Et₂O, room temp., 5 min, 2.) Et₂O, -60 deg C, 6 h

2: 100 percent / pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; diethylaluminium chloride; In dichloromethane;
DOI:10.1021/jo971913n

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 204127-03-7
(2S,3S)-N-benzyl-3-(acetoxyamino)-1,2-O-isopropylidene-3-phenyl-1,2-propanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₂AlCl / 1.) Et₂O, room temp., 5 min, 2.) Et₂O, -60 deg C, 6 h

2: 100 percent / pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; diethylaluminium chloride; In dichloromethane;
DOI:10.1021/jo971913n