(2Z,4R)-2--4,5-diphenyl-2-pentenenitrile

Base Information

• Chemical Name: (2Z,4R)-2--4,5-diphenyl-2-pentenenitrile
• CAS No.: 127393-09-3
• Molecular Formula: C₂₇H₂₈N₂O
• Molecular Weight: 396.532

Synonyms:(2Z,4R)-2--4,5-diphenyl-2-pentenenitrile

Chemical Property of (2Z,4R)-2--4,5-diphenyl-2-pentenenitrile

Chemical Property:

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Technology Process of (2Z,4R)-2--4,5-diphenyl-2-pentenenitrile

There total 2 articles about (2Z,4R)-2--4,5-diphenyl-2-pentenenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) + 2--4-phenyl-3-butenenitrile → (2Z,4R)-2--4,5-diphenyl-2-pentenenitrile (127393-09-3)

Guidance literature:

With lithium iodide; lithium diisopropyl amide; Yield given. Multistep reaction; 1) THF, -78 deg C, 2) THF, -78 deg C, 20 min;

DOI:10.1021/jo00059a027

Reference yield:

benzyl bromide (100-39-0) + 2--4-phenyl-3-butenenitrile → (2Z,4R)-2--4,5-diphenyl-2-pentenenitrile (127393-09-3) + (2E,4R)-2--4,5-diphenyl-2-pentenenitrile + (2E,4S)-2--4,5-diphenyl-2-pentenenitrile

Guidance literature:

With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1) THF, -78 deg C, 2) THF, -78 deg C to room temperature, 3 h;

DOI:10.1021/jo00059a027

Reference yield:

(2Z,4R)-2--4,5-diphenyl-2-pentenenitrile (127393-09-3) → (R)-3,4-diphenyl butanoic acid (6995-48-8)

Guidance literature:

With oxalic acid; In tetrahydrofuran; at 100 ℃; for 12h;

DOI:10.1021/jo00059a027

upstream raw materials:

benzyl bromide

Downstream raw materials:

(R)-3,4-diphenyl butanoic acid

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