(4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

Base Information

Chemical Name:(4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone
CAS No.:212501-50-3
Molecular Formula:C₂₆H₂₈O₆
Molecular Weight:436.505
Hs Code.:

Synonyms:(4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

Chemical Property:

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Technology Process of (4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

There total 1 articles about (4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1011-27-4
3,5-dimethoxy-4-methylbenzaldehyde

: 81418-49-7
5-(benzyloxy)-2-bromobenzaldehyde dimethylacetal

: 212501-50-3
(4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

Guidance literature:: 5-(benzyloxy)-2-bromobenzaldehyde dimethylacetal; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

3,5-dimethoxy-4-methylbenzaldehyde; In tetrahydrofuran; at -78 ℃; for 0.5h; Further stages.;
DOI:10.1021/jm000558h

Reference yield:

: 212501-50-3
(4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

: 1027587-99-0
5-benzyloxy-2-(3,5-dimethoxy-4-methyl-benzoyl)-benzaldehyde

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1021/jm000558h

Reference yield:

: 212501-50-3
(4-benzyloxy-2-dimethoxymethyl-phenyl)-(3,5-dimethoxy-4-methyl-phenyl)-methanone

: 212499-73-5
2-(4-tert-butoxycarbonylamino-phenyl)-4-(3,5-dimethoxy-4-methyl-phenyl)-7-hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: TFA / CH₂Cl₂; H₂O / 2 h / 20 °C

2.1: resorcinol; acetate buffer; NaClO₂ / dioxane; H₂O / 20 °C / pH 3.8

3.1: K₂CO₃ / dimethylformamide / 20 °C

4.1: 4 N HCl / ethyl acetate / 20 °C

4.2: AcOH / dioxane / 6 h / Heating

5.1: 2 N aq. NaOH / tetrahydrofuran; methanol / 2 h / 20 °C

6.1: i-Pr₂NEt / various solvent(s) / 8 h / 110 °C

7.1: K₂CO₃ / dimethylformamide / 0.5 h / 20 °C

8.1: H₂ / 10percent Pd/C / tetrahydrofuran; methanol / 20 °C

With hydrogenchloride; sodium hydroxide; sodium chlorite; acetate buffer; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; recorcinol; 10percent Pd/C; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm000558h