(4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

Base Information

Chemical Name:(4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate
CAS No.:1357918-36-5
Molecular Formula:C₇H₇O₃S*C₁₆H₁₇ClIO₃
Molecular Weight:590.863
Hs Code.:

Synonyms:(4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

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Chemical Property of (4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

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Technology Process of (4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

There total 2 articles about (4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54589-53-6
4-iodobenzyl chloride

: 1357918-36-5
(4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: -10 - 20 °C

2: water / acetonitrile

3: chloroform; acetonitrile / 4 h / Acidic conditions; Reflux

With water; In chloroform; acetonitrile;
DOI:10.1021/jo202517v

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: C₁₄H₁₄ClIO₄S

: 1357918-36-5
(4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

Guidance literature:: In chloroform; acetonitrile; for 4h; regiospecific reaction; Acidic conditions; Reflux;
DOI:10.1021/jo202517v

Reference yield: 52.0%

: 1357918-36-5
(4-chloromethylphenyl)(2’,4’,6’-trimethoxyphenyl)iodonium tosylate

: 1376770-05-6
C₇H₆Cl⁽¹⁸⁾F

: 1453864-86-2
[¹⁸F]-2-fluoro-1,3,5-trimethoxybenzene

Guidance literature:: With K[18F]F-4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane complex; In N,N-dimethyl-formamide; at 180 ℃; for 0.0522222h;
DOI:10.1039/c3ob41353e