2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

Base Information

Chemical Name:2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene
CAS No.:1273542-60-1
Molecular Formula:C₁₈H₁₉Br₃O₄
Molecular Weight:539.058
Hs Code.:

Synonyms:2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

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Chemical Property of 2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

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Technology Process of 2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

There total 2 articles about 2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 68278-85-3
3-bromo-4,5-dimethoxy-toluene

: 4950-08-7
(2,3-dibromo-4,5-dimethoxyphenyl)methanol

: 1273542-60-1
2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/j.ejmech.2013.03.037

Reference yield:

: 70625-29-5
2,3-dibromo-4,5-dimethoxybenzaldehyde

: 1273542-60-1
2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium tetrahydroborate / Cooling with ice

2: aluminum (III) chloride / dichloromethane / Cooling with ice

With methanol; aluminum (III) chloride; sodium tetrahydroborate; In dichloromethane;

Reference yield:

: 1273542-60-1
2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene

: 1238891-85-4
{3-bromo-2-[(2,3-dibromo-4,5-dimethoxyphenyl)methyl]-4,5-dimethoxyphenyl}methanol

Guidance literature:: 2,3-dibromo-1-(2'-bromo-3',4'-dimethoxy-6'-methylbenzyl)-4,5-dimethoxy benzene; With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; Irradiation;

With potassium carbonate; In 1,4-dioxane; water; at 90 ℃;
DOI:10.3390/md11020350