Technology Process of C31H34N2O4
There total 4 articles about C31H34N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; DavePhos;
In
1,4-dioxane;
at 100 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethyl ether / 1.25 h / 60 - 200 °C / Inert atmosphere
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 35 °C
3: tris-(dibenzylideneacetone)dipalladium(0); DavePhos; caesium carbonate / 1,4-dioxane / 16 h / 100 °C
With
tris-(dibenzylideneacetone)dipalladium(0); oxalyl dichloride; caesium carbonate; N,N-dimethyl-formamide; DavePhos;
In
1,4-dioxane; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydrogencarbonate; iodine / dichloromethane; water / 1.5 h / 0 °C
2: copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; caesium carbonate / toluene / 23 h / 80 - 110 °C / Inert atmosphere
3: diethyl ether / 1.25 h / 60 - 200 °C / Inert atmosphere
4: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 35 °C
5: tris-(dibenzylideneacetone)dipalladium(0); DavePhos; caesium carbonate / 1,4-dioxane / 16 h / 100 °C
With
tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; oxalyl dichloride; 3,4,7,8-Tetramethyl-o-phenanthrolin; iodine; sodium hydrogencarbonate; caesium carbonate; N,N-dimethyl-formamide; DavePhos;
In
1,4-dioxane; diethyl ether; dichloromethane; water; toluene;