11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one

Base Information

• Chemical Name: 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one
• CAS No.: 1253388-70-3
• Molecular Formula: C₃₆H₂₅NO₂
• Molecular Weight: 503.6
• Mol file: 1253388-70-3.mol

Synonyms:11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one

Chemical Property of 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one

There total 7 articles about 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

6-methoxy-2,3-diphenylisoquinolin-1(2H)-one (1225462-91-8) + diphenyl acetylene (501-65-5) → 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one (1253388-70-3)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In o-xylene; at 120 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201203374

Reference yield: 86.0%

4-methoxyphenylacetamide (3424-93-9) + diphenyl acetylene (501-65-5) → 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one (1253388-70-3)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate; In acetonitrile; at 115 ℃; for 10h; Inert atmosphere;

DOI:10.1021/jo101596d

Reference yield: 52.0%

4-methoxy-N-(naphthalen-1-yl)benzamide (63295-63-6) + diphenyl acetylene (501-65-5) → 11-methoxy-5,6,13-triphenyl-8H-isoquinolino[3,2-a]isoquinolin-8-one (1253388-70-3)

Guidance literature:

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) acetate; In acetonitrile; at 80 ℃; for 12h;

DOI:10.1002/cctc.201500410

upstream raw materials:

4-methoxyphenylacetamide

diphenyl acetylene

6-methoxy-2,3-diphenylisoquinolin-1(2H)-one

4-methoxy-N-(naphthalen-1-yl)benzamide