(S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

Base Information

Chemical Name:(S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine
CAS No.:672314-41-9
Molecular Formula:C₂₂H₃₇NOSi
Molecular Weight:359.627
Hs Code.:

Synonyms:(S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

Suppliers and Price of (S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

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Technology Process of (S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

There total 4 articles about (S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 141836-47-7
4-(((tert-butyldimethylsilyl)oxy)methyl)cyclohexane carbaldehyde

: 672314-41-9
(S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃;

Reference yield:

: 105-08-8
bis-1,4-(hydroxymethyl)cyclohexane

: 672314-41-9
(S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / Et₃N; DMAP

2: 80 percent / PCC / CH₂Cl₂

3: MgSO₄ / CH₂Cl₂

With dmap; magnesium sulfate; triethylamine; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/j.bmcl.2004.07.025

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 672314-41-9
(S)-N-[(4'-tert-butyldimethylsilyloxymethyl-cyclohexyl)methylidene]-1-phenylethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / Et₃N; DMAP

2: 80 percent / PCC / CH₂Cl₂

3: MgSO₄ / CH₂Cl₂

With dmap; magnesium sulfate; triethylamine; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/j.bmcl.2004.07.025