benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

Base Information

Chemical Name:benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate
CAS No.:1380351-14-3
Molecular Formula:C₂₈H₃₆N₆O₅
Molecular Weight:536.631
Hs Code.:

Synonyms:benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

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Chemical Property of benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

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Technology Process of benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

There total 3 articles about benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21950-36-7
5'-amino-5'-deoxy-2',3'-O-isopropylideneadenosine

: 1380351-14-3
benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / isopropyl alcohol; 1,2-dichloro-ethane / 1 h / 20 °C

1.2: 18 h

2.1: potassium carbonate / acetonitrile / 18 h / 95 °C / Sealed tube

3.1: water; methanol / 0.75 h

3.2: 2 h / 20 °C

With potassium carbonate; acetic acid; In methanol; water; 1,2-dichloro-ethane; isopropyl alcohol; acetonitrile;

Reference yield:

: 1380351-08-5
benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}amino)cyclobutyl]propanoate

: 1380351-14-3
benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 18 h / 95 °C / Sealed tube

2.1: water; methanol / 0.75 h

2.2: 2 h / 20 °C

With potassium carbonate; In methanol; water; acetonitrile;

Reference yield:

: 1380291-49-5
3-(3-oxo-cyclobutyl)-propionic acid benzyl ester

: 1380351-14-3
benzyl 3-[3-({[(3aR,4R,6R,6aR)-6-(6-amino-9H-purin-9-yl)-2,2-dimethyl-tetrahydro-2H-furo[3,4-d][1,3]dioxol-4-yl]methyl}(methyl)amino)cyclobutyl]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / isopropyl alcohol; 1,2-dichloro-ethane / 1 h / 20 °C

1.2: 18 h

2.1: potassium carbonate / acetonitrile / 18 h / 95 °C / Sealed tube

3.1: water; methanol / 0.75 h

3.2: 2 h / 20 °C

With potassium carbonate; acetic acid; In methanol; water; 1,2-dichloro-ethane; isopropyl alcohol; acetonitrile;