C₁₃H₁₅NOS

Base Information

• Chemical Name: C₁₃H₁₅NOS
• CAS No.: 1021058-80-9
• Molecular Formula: C₁₃H₁₅NOS
• Molecular Weight: 233.334
• Mol file: 1021058-80-9.mol

Synonyms:C₁₃H₁₅NOS

Chemical Property of C₁₃H₁₅NOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₃H₁₅NOS

There total 3 articles about C₁₃H₁₅NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-methoxy-N-(1-(thiophen-2-yl)ethylidene)benzenamine → C13H15NOS (1021058-80-9)

Guidance literature:

With phenylsilane; C₁₂H₃₇CoP₄⁽¹⁺⁾; In toluene; at 110 ℃; for 1h;

DOI:10.1021/acscatal.1c03886

Reference yield: 82.0%

2-Acetylthiophene (88-15-3,97511-16-5) + 4-methoxy-aniline (104-94-9) → C13H15NOS (1021058-80-9)

Guidance literature:

With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; In neat (no solvent); at 150 ℃; for 24h; Molecular sieve;

DOI:10.1016/j.tet.2013.04.046

Reference yield:

4-methoxy-aniline (104-94-9) → C13H15NOS (1021058-80-9)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / 72 h / Molecular sieve; Inert atmosphere

2: sodium tetrahydroborate / ethanol / 24 h / Inert atmosphere

With sodium tetrahydroborate; In ethanol; benzene;

DOI:10.1021/acs.orglett.0c00887

upstream raw materials:

2-Acetylthiophene

4-methoxy-aniline