Technology Process of C13H14O3
There total 5 articles about C13H14O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1039/c3ob27491h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
With
n-butyllithium; tetrabutyl ammonium fluoride; acetic acid; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c3ob27491h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
With
triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; acetic acid; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c3ob27491h
