4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine

Base Information

• Chemical Name: 4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine
• CAS No.: 1416235-95-4
• Molecular Formula: C₇₁H₅₉N₇O₆Ru
• Molecular Weight: 1207.36

Synonyms:4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine

Chemical Property of 4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine

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Technology Process of 4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine

There total 1 articles about 4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

4'-(2-{2-[2-(tosylate-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine (1416235-89-6) + ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin (1416235-92-1) → 4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine (1416235-95-4)

Guidance literature:

ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin; With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

4'-(2-{2-[2-(tosylate-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine; In N,N-dimethyl-formamide; at 70 ℃; for 72h;

DOI:10.1039/c2ob26587g

Reference yield:

iron(II) tetrafluoroborate tetrahydrate + 4'-(2-{2-[2-(ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine (1416235-95-4) + 2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-(2,2':6',2''-terpyridine)ethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide (1416235-68-1) → C122H111FeN13O19Ru(2+)*2BF4(1-)

Guidance literature:

In d⁽⁴⁾-methanol; dichloromethane-d2;

DOI:10.1039/c2ob26587g

upstream raw materials:

4'-(2-{2-[2-(tosylate-2-ethoxy)ethoxy]ethoxy}ethoxy)-2,2':6',2''-terpyridine

ruthenium(II) carbonyl 5-[m-hydroxyphenyl]-10,15,20-tris-[p-tolyl]porphyrin

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