tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)

Base Information

Chemical Name:tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)
CAS No.:116785-35-4
Molecular Formula:C₄₅H₃₃Cu₃N₆
Molecular Weight:848.435
Hs Code.:

Synonyms:tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)

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Chemical Property of tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)

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Technology Process of tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)

There total 2 articles about tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 1145-01-3
3,5-Diphenylpyrazole

: 116785-35-4
tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)

Guidance literature:: With Et₃N; In acetone; stirring of Cu(CH3CN)4PF6 and 3,5-diphenylpyrazole in acetone; addn. dropwise of Et3N; pptn., stirring for 30 min; filtration, washing with acetone, drying in vac.;
DOI:10.1016/j.ica.2004.03.016

Reference yield:

: sodium 3,5-diphenylpyrazolate

: 111495-79-5
tris(μ-3,5-diphenylpyrazolato-N,N')trisilver(I)

: 116785-35-4
tris(μ-3,5-diphenylpyrazolato-N,N')tricopper(I)

Guidance literature:: With copper(I) chloride;; silver nitrate;; In dichloromethane; 16 h; recrystn. from methylene dichloride/ diethyl ether at -5°C;; MS;;