C--N-(triphenylsilyl)nitrilimine

Base Information

Chemical Name:C--N-(triphenylsilyl)nitrilimine
CAS No.:116889-37-3
Molecular Formula:C₃₁H₄₃N₄PSSi
Molecular Weight:562.834
Hs Code.:

C-<bis(diisopropylamino)thiophosphoranyl>-N-(triphenylsilyl)nitrilimine

Synonyms:C--N-(triphenylsilyl)nitrilimine

Suppliers and Price of C--N-(triphenylsilyl)nitrilimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C--N-(triphenylsilyl)nitrilimine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C--N-(triphenylsilyl)nitrilimine

There total 3 articles about C--N-(triphenylsilyl)nitrilimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-86-8
Triphenylsilyl chloride

: 113597-81-2
diazomethane

: 116889-37-3
C--N-(triphenylsilyl)nitrilimine

Guidance literature:: With n-butyllithium; Multistep reaction; 1) -78 deg C, 10 min, THF, hexane, 2) -78 deg C;
DOI:10.1021/jo00005a026

Reference yield:

: 113533-22-5
C--N-nitrilimine

: 116889-37-3
C--N-(triphenylsilyl)nitrilimine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / SiO₂ / H₂O

2: 1.) BuLi/n-hexane / 1.) THF, -78 deg C, 30 min; 2.) THF, -40 deg C

With n-butyllithium; hexane; silica gel; In water;

Reference yield:

: 116889-36-2
C--N-(trimethylsilyl)nitrilimine

: 116889-37-3
C--N-(triphenylsilyl)nitrilimine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₃OH

2: 1.) BuLi/n-hexane / 1.) THF, -78 deg C, 30 min; 2.) THF, -40 deg C

With methanol; n-butyllithium; hexane;