C₁₃H₁₅IO₃

Base Information

Chemical Name:C₁₃H₁₅IO₃
CAS No.:1334288-77-5
Molecular Formula:C₁₃H₁₅IO₃
Molecular Weight:346.165
Hs Code.:

C<sub>13</sub>H<sub>15</sub>IO<sub>3</sub>

Synonyms:C₁₃H₁₅IO₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₅IO₃

Chemical Property:

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Technology Process of C₁₃H₁₅IO₃

There total 10 articles about C₁₃H₁₅IO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334288-87-7
C₁₃H₁₇IO₃

: 1334288-77-5
C₁₃H₁₅IO₃

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; for 1.5h;
DOI:10.1016/j.tet.2011.07.066

Reference yield:

: 1179989-36-6
C₁₂H₁₄O₄

: 1334288-77-5
C₁₃H₁₅IO₃

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / methanol / 1.17 h / 0 - 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / tetrahydrofuran / 0.33 h

3: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C

4: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.07.066

Reference yield:

: 1179989-35-5
C₁₂H₁₆O₄

: 1334288-77-5
C₁₃H₁₅IO₃

Guidance literature:: Multi-step reaction with 5 steps

1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

2: potassium carbonate / methanol / 1.17 h / 0 - 20 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / tetrahydrofuran / 0.33 h

4: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C

5: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.07.066