ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

Base Information

Chemical Name:ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate
CAS No.:1033434-95-5
Molecular Formula:C₂₀H₁₉N₃O₃
Molecular Weight:349.389
Hs Code.:

Synonyms:ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

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Chemical Property of ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

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Technology Process of ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

There total 2 articles about ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1033434-94-4
8-iodo-7-ethoxycarbonylamino-2-methylimidazo[1,2-a]pyridine

: 768-60-5
4-methoxyphenylacetylen

: 1033434-95-5
ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;

Reference yield: 25.0%

: 1033434-94-4
8-iodo-7-ethoxycarbonylamino-2-methylimidazo[1,2-a]pyridine

: 2749-94-2
1-methoxy-4-(prop-1-yn-1-yl)benzene

: 1033434-95-5
ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.09.056

Reference yield: 35.0%

: 1033434-95-5
ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate

: 1033435-00-5
8-(4-methoxyphenyl)-2-methylimidazo[1,2-a]pyrrolo[3,2-c]pyridine

Guidance literature:: ethyl [8-[2-(4-methoxyphenyl)ethynyl]-2-methylimidazo[1,2-a]pyridine-7-yl]carbamate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 20h; Reflux;

With sodium carbonate; In tetrahydrofuran; water; pH=12;