5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

Base Information

Chemical Name:5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline
CAS No.:122509-57-3
Molecular Formula:C₁₃H₁₅N₃O₆S
Molecular Weight:341.345
Hs Code.:

5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ<sup>4</sup>-isoxazoline

Synonyms:5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

Suppliers and Price of 5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

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Technology Process of 5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

There total 2 articles about 5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 72552-73-9
N-2-propylidenemethanamide N-oxide

: 122509-56-2
<(2,4-dinitrophenyl)sulfinyl>-1,2-propadiene

: 122509-57-3
5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

Guidance literature:: In dichloromethane; at 50 ℃; for 4h;
DOI:10.1021/jo00013a033

Reference yield:

: 528-76-7
2,4-dinitrobenzenesulfenyl chloride

: 122509-57-3
5-<<(2,4-dinitrophenyl)sulfenyloxy>methyl>-2-methyl-3-phenyl-Δ⁴-isoxazoline

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / CH₂Cl₂ / 0.17 h / -95 °C

2: 98 percent / CH₂Cl₂ / 4 h / 50 °C

With triethylamine; In dichloromethane;
DOI:10.1021/jo00013a033