2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

Base Information

Chemical Name:2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide
CAS No.:674773-25-2
Molecular Formula:C₂₁H₂₄N₂O₃
Molecular Weight:352.433
Hs Code.:

Synonyms:2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

Chemical Property:

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Technology Process of 2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

There total 7 articles about 2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-formylamino-N-[2-(3-methoxy-4-prop-2-ynyloxy-phenyl)-ethyl]-2-p-tolyl-acetamide

: 674773-25-2
2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

Guidance literature:: With hydrogenchloride; In ethanol;
DOI:10.2533/000942903777678542

Reference yield:

: 22568-51-0
(E)-2-methoxy-4-(2-nitrovinyl)phenol

: 674773-25-2
2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

Guidance literature:: Multi-step reaction with 7 steps

1: NaBH₄

2: H₂ / Pd/C

3: 54 percent / Ac₂O

4: 98 percent / NaOMe

5: 81 percent / POCl₃; Et₃N

6: HCl / ethanol

With hydrogenchloride; sodium tetrahydroborate; hydrogen; sodium methylate; acetic anhydride; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol; 6: Ugi reaction;
DOI:10.2533/000942903777678542

Reference yield:

: 528594-30-1
2-methoxy-4-(2-nitroethyl)phenol

: 674773-25-2
2-amino-N-[2-(3-methoxy-4-(prop-2-ynyloxy)phenyl)ethyl]-2-p-tolylacetamide

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / Pd/C

2: 54 percent / Ac₂O

3: 98 percent / NaOMe

4: 81 percent / POCl₃; Et₃N

5: HCl / ethanol

With hydrogenchloride; hydrogen; sodium methylate; acetic anhydride; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol; 5: Ugi reaction;
DOI:10.2533/000942903777678542