Technology Process of C20H16N2O2
There total 8 articles about C20H16N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; 4 A molecular sieve; copper diacetate;
In
DMF (N,N-dimethyl-formamide);
at 80 ℃;
- Guidance literature:
-
With
4 A molecular sieve;
copper diacetate;
In
pyridine; DMF (N,N-dimethyl-formamide);
for 80h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydroxylamine; sodium acetate / ethanol; water / 2.5 h / Heating / reflux
2.1: acetic acid / 2 h / Heating / reflux
3.1: N,N-dimethyl-formamide; trichlorophosphate / 0.5 h / 0 °C
3.2: 0 - 20 °C
4.1: hydrogen; triethylamine / palladium 10% on activated carbon / tetrahydrofuran / 2 h
5.1: 3-chloro-benzenecarboperoxoic acid / ethanol / 2 h / Heating / reflux
5.2: 0.5 h / Heating / reflux
6.1: 4 A molecular sieve / copper diacetate / pyridine; DMF (N,N-dimethyl-formamide) / 80 h
With
4 A molecular sieve; hydrogen; hydroxylamine; sodium acetate; triethylamine; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate;
palladium 10% on activated carbon; copper diacetate;
In
tetrahydrofuran; pyridine; DMF (N,N-dimethyl-formamide); ethanol; water; acetic acid;