dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

Base Information

Chemical Name:dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate
CAS No.:1428550-18-8
Molecular Formula:C₂₆H₂₉NO₆S
Molecular Weight:483.585
Hs Code.:

Synonyms:dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

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Chemical Property of dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

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Technology Process of dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

There total 4 articles about dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1428549-90-9
dimethyl 2-(4-methyl-N-(1-phenylhept-2-ynyl)phenylsulfonamido)maleate

: 1428550-18-8
dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

Guidance literature:: In methanol; at 60 ℃; for 66h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1021/jo400387b

Reference yield:

: 1372628-26-6
dimethyl 2-(4-methyl-N-(1-phenylhept-2-ynyl)phenylsulfonamido)maleate

: 1428550-18-8
dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

Guidance literature:: In ethanol; at 70 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2013.10.038

Reference yield:

: 762-42-5
dimethyl acetylenedicarboxylate

: 1428550-18-8
dimethyl 4-butyl-6-phenyl-1-tosyl-1,6-dihydropyridine-2,3-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / dichloromethane / Inert atmosphere; Schlenk technique

2: methanol / 66 h / 60 °C / Inert atmosphere; Schlenk technique; Sealed tube

With caesium carbonate; In methanol; dichloromethane;
DOI:10.1021/jo400387b