4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

Base Information

Chemical Name:4-dibenzylamino-1-methyl-1,2,4-triazolium triflate
CAS No.:873589-87-8
Molecular Formula:CF₃O₃S*C₁₇H₁₉N₄
Molecular Weight:428.435
Hs Code.:

Synonyms:4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

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Chemical Property of 4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

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Technology Process of 4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

There total 2 articles about 4-dibenzylamino-1-methyl-1,2,4-triazolium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 333-27-7
methyl trifluoromethanesulfonate

: 6085-96-7
dibenzyl-[1,2,4]triazol-4-yl-amine

: 873589-87-8
4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.jorganchem.2005.07.120

Reference yield:

: 5802-60-8
N,N-dibenzylhydrazine

: 873589-87-8
4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / pyridine / 4 h / 100 °C

2: 87 percent / CH₂Cl₂ / 1 h / 20 °C

In pyridine; dichloromethane;
DOI:10.1016/j.jorganchem.2005.07.120

Reference yield: 64.0%

: 873589-87-8
4-dibenzylamino-1-methyl-1,2,4-triazolium triflate

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: [Rh(COD)Cl(4-dibenzylamino-1-methyl-1,2,4-triazol-5-ylidene)]

Guidance literature:: With (C₂H₅)3N; In tetrahydrofuran; addn. of Et3N to suspn. of 4-dibenzylamino-2-methyl-1,2,4-triazolium triflate and (Rh(COD)Cl)2 in THF; stirring for 1 h at room temp.; removal of solvent in vac., flash chromy. (AcOEt-Hex 1:4); elem. anal.;
DOI:10.1016/j.jorganchem.2005.07.120