ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

Base Information

Chemical Name:ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate
CAS No.:153780-29-1
Molecular Formula:C₂₁H₃₀N₂O₆S
Molecular Weight:438.545
Hs Code.:

Synonyms:ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

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Chemical Property of ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

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Technology Process of ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

There total 3 articles about ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3,3-Diethoxy-2-{[1-[1-(toluene-4-sulfonyl)-1H-pyrrol-2-yl]-meth-(Z)-ylidene]-amino}-propionic acid ethyl ester

: 153780-29-1
ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

Guidance literature:: With sodium cyanoborohydride; In ethanol; at 0 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)88033-9

Reference yield:

: 61040-21-9
ethyl 2-amino-3,3-diethoxypropanoate

: 153780-29-1
ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 4 Angstroem molecular sieves / CH₂Cl₂ / 48 h / Ambient temperature

2: 95 percent / NaBH₃CN / ethanol / 0.17 h / 0 °C

With 4 A molecular sieve; sodium cyanoborohydride; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)88033-9

Reference yield:

: 102619-05-6
1-(toluene-4-sulfonyl)-1H-pyrrole-2-carbaldehyde

: 153780-29-1
ethyl 2-<1-(p-toluenesulfonylpyrrol-2-yl)methyl>amino-3,3-diethoxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 4 Angstroem molecular sieves / CH₂Cl₂ / 48 h / Ambient temperature

2: 95 percent / NaBH₃CN / ethanol / 0.17 h / 0 °C

With 4 A molecular sieve; sodium cyanoborohydride; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)88033-9