N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide

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Chemical Name:N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide
CAS No.:215297-20-4
Molecular Formula:C₅₉H₅₈N₂O₁₀Si
Molecular Weight:983.202
Hs Code.:

Synonyms:N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide

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Chemical Property of N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide

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Technology Process of N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide

There total 2 articles about N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 215297-19-1
N-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-N'-2-(2-hydroxyethoxy)ethyl-3,4,9,10-perylenetetracarboxylic diimide

: 215297-20-4
N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide

Guidance literature:: With pyridine; for 3h;
DOI:10.1021/ja0001714

Reference yield:

: 215297-18-0
N,N'-bis(2-(2-dimethyl-tert-butylsilyloxyethoxy)ethyl)perylene-3,4,9,10-tetracarboxylic acid bisimide

: 215297-20-4
N-[2-(2-O-4,4'-dimethoxytritylethoxy)ethyl]-N'-[2-(2-O-tert-butyldimethylsilylethoxy)ethyl]-3,4,9,10-perylenetetracarboxylic diimide

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / HF; pyridine

2: 69 percent / pyridine / 3 h

With pyridine; hydrogen fluoride; 1: desilylation / 2: tritylation;
DOI:10.1021/ja0001714