Mirogabalin besylate

Base Information

Chemical Name:Mirogabalin besylate
CAS No.:1138245-21-2
Molecular Formula:C₆H₆O₃S*C₁₂H₁₉NO₂
Molecular Weight:367.466
Hs Code.:
Mol file:1138245-21-2.mol

Synonyms:[(1R,5S,6S)-6-(Aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]acetic acid monobenzenesulfonate

Suppliers and Price of Mirogabalin besylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

DC Chemicals
Mirogabalinbesylate >98%
250 mg
$ 900.00

ChemScene
Mirogabalinbesylate 99.98%
100mg
$ 750.00

ChemScene
Mirogabalinbesylate 99.98%
50mg
$ 490.00

ChemScene
Mirogabalinbesylate 99.98%
10mg
$ 190.00

ChemScene
Mirogabalinbesylate 99.98%
5mg
$ 120.00

Chemenu
2-[(1R,5S,6S)-6-(aminomethyl)-3-ethyl-6-bicyclo[3.2.0]hept-3-enyl]aceticacid;benzenesulfonicacid 95%+
100g
$ 4375.00

Total 68 raw suppliers

Chemical Property of Mirogabalin besylate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Mirogabalinbesylate >98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Mirogabalin besylate

There total 10 articles about Mirogabalin besylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1138245-13-2
DS-5565

: 98-11-3
benzenesulfonic acid

: 1138245-21-2
[(1R,5S,6S)-6-(Aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]acetic acid monobenzenesulfonate

Guidance literature:: In water; Heating;

Reference yield:

: diethyl [(1R,5S)-3-ethylbicyclo[3.2.0]hept-3-en-6-ylidene]propanedioate

: 1138245-21-2
[(1R,5S,6S)-6-(Aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]acetic acid monobenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 4 h / 20 °C

2.1: potassium hydroxide / ethanol; water / 10 h / 20 °C / Reflux

2.2: 10 - 20 °C

3.1: hydrogenchloride / water; tert-butyl methyl ether / 20 °C

3.3: sponge cobalt; dimethylpolysiloxane / 7.5 h / 40 °C / 3375.34 Torr

4.1: acetone; water; tert-butyl methyl ether / 4.5 h / -10 - 20 °C

With hydrogenchloride; potassium hydroxide; In ethanol; tert-butyl methyl ether; water; acetone;

Reference yield:

: diethyl [(1R,5S,6R)-6-cyano-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]propanedioate

: 1138245-21-2
[(1R,5S,6S)-6-(Aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]acetic acid monobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol; water / 10 h / 20 °C / Reflux

1.2: 10 - 20 °C

2.1: hydrogenchloride / water; tert-butyl methyl ether / 20 °C

2.3: sponge cobalt; dimethylpolysiloxane / 7.5 h / 40 °C / 3375.34 Torr

3.1: acetone; water; tert-butyl methyl ether / 4.5 h / -10 - 20 °C

With hydrogenchloride; potassium hydroxide; In ethanol; tert-butyl methyl ether; water; acetone;