Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

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Chemical Name:Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄
CAS No.:174581-95-4
Molecular Formula:C₃₃H₂₆N₅ORu*ClO₄
Molecular Weight:709.123
Hs Code.:

Ru(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2(C<sub>6</sub>H<sub>4</sub>OCHNC<sub>6</sub>H<sub>5</sub>)<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[Ru(C<sub>10</sub>H<sub>8</sub>N<sub>2</sub>)2(C<sub>6</sub>H<sub>4</sub>OCHNC<sub>6</sub>H<sub>5</sub>)]ClO<sub>4</sub>

Synonyms:Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

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Chemical Property of Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

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Technology Process of Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

There total 2 articles about Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: bis(2,2'-bipyridine)dichlororuthenium(II) dihydrate

: 779-84-0,103886-91-5,103886-92-6
salicylidene aniline

: sodium perchlorate

: 174581-95-4
Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

Guidance literature:: bis(2,2'-bipyridine)dichlororuthenium(II) dihydrate; With silver nitrate; In ethanol; for 0.666667h; Reflux;

salicylidene aniline; In ethanol; for 6h; Reflux;

sodium perchlorate; In water; at 20 ℃;
DOI:10.1080/00958972.2018.1469749

Reference yield: 78.0%

: 345911-20-8,19542-80-4,158060-65-2,34795-02-3,15746-57-3
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)

N-phenylsalicylaldimine: 779-84-0
N-phenylsalicylaldimine

: sodium perchlorate

: 174581-95-4
Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

Guidance literature:: With AgNO₃; CH₃COONa; In ethanol; byproducts: AgCl; stirring (Ru complex with AgNO3, 30 min), filtration, ligand addn., NaOAc addn., reflux (1 h, water bath), cooling (room temp.), NaClO4 addn. (pptn.); washing (cold water) drying (vacuum, P4O10), recrystn. (acetonitrile/benzene, 1:1); elem. anal.;
DOI:10.1016/0277-5387(95)00362-2

Reference yield: 84.0%

: 174581-95-4
Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽¹⁺⁾*ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)]ClO₄

: Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)⁽²⁺⁾*2ClO₄^(1-)=[Ru(C₁₀H₈N₂)2(C₆H₄OCHNC₆H₅)](ClO₄)2

Guidance literature:: With ammonium ceric sulphate; NaClO₄; In water; acetonitrile; stirring (10 min), filtration, NaClO4 addn., partial solvent evapn. (pptn.); washing (cold water) drying (vacuum, P4O10); elem. anal.;
DOI:10.1016/0277-5387(95)00362-2