N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide
• CAS No.: 1269207-66-0
• Molecular Formula: C₁₅H₁₄Cl₂N₂O₂S
• Molecular Weight: 357.26
• Mol file: 1269207-66-0.mol

Synonyms:N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Chemical Property of N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

toluene-4-sulfonic acid hydrazide (1576-35-8) + 1-(2,4-dichlorophenyl)ethan-1-one (2234-16-4) → N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1269207-66-0)

Guidance literature:

In methanol; Reflux;

DOI:10.1021/ja111249p

Reference yield: 92.0%

N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1269207-66-0) + (E)-3-(N,N-dimethylamino)-1-phenyl-2-propen-1-one (1131-80-2,1201-93-0,31919-75-2) → 2-(2,4-dichlorophenyl)-2-methyl-4-oxo-4-phenylbutanal

Guidance literature:

With copper hydroxide; potassium carbonate; In toluene; at 80 ℃; for 24h; regioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1039/c7cc07178g

Reference yield: 86.0%

1,3-Benzothiazole (95-16-9) + N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1269207-66-0) → 2-(1-(2,4-dichlorophenyl)ethyl)benzo[d]thiazole (1269207-20-6)

Guidance literature:

With copper(l) iodide; lithium tert-butoxide; In 1,4-dioxane; at 120 ℃; for 1h; Inert atmosphere;

DOI:10.1021/ja111249p

upstream raw materials:

toluene-4-sulfonic acid hydrazide

1-(2,4-dichlorophenyl)ethan-1-one

Downstream raw materials:

2-(1-(2,4-dichlorophenyl)ethyl)-4,5-dimethylthiazole

2-(1-(2,4-dichlorophenyl)ethyl)benzo[d]thiazole

N-(1-(2,4-dichlorophenyl)ethyl)-N'-(1-(2,4-dichlorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide

1-(1-(2,4-dichlorophenyl)vinyl)-1H-indole