E-3--1-(naphth-1-yl)prop-1-ene

Base Information

Chemical Name:E-3--1-(naphth-1-yl)prop-1-ene
CAS No.:223394-04-5
Molecular Formula:C₂₅H₂₅NO
Molecular Weight:355.48
Hs Code.:

E-3-<N-(benzoyl)piperidin-4-yl>-1-(naphth-1-yl)prop-1-ene

Synonyms:E-3--1-(naphth-1-yl)prop-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of E-3--1-(naphth-1-yl)prop-1-ene

Chemical Property:

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Technology Process of E-3--1-(naphth-1-yl)prop-1-ene

There total 7 articles about E-3--1-(naphth-1-yl)prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5344-27-4
4-(2-hydroxyethyl)pyridine

: 223394-04-5
E-3--1-(naphth-1-yl)prop-1-ene

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / H₂, conc. HCl / Pt/C / H₂O / 264 h / Ambient temperature

2: 98 percent / 4M NaOH / Ambient temperature

3: (COCl)2, DMSO, Et₃N / tetrahydrofuran / 0.5 h / -35 - 20 °C

4: 1.) nBuLi / 1.) THF, hexane, room temperature, 30 min, 2.) THF, -78 deg C -> room temperature, 2 h

5: PhSSPh / CHCl₃ / 240 h / Irradiation

With hydrogenchloride; sodium hydroxide; n-butyllithium; oxalyl dichloride; hydrogen; dimethyl sulfoxide; triethylamine; diphenyldisulfane; platinum on activated charcoal; In tetrahydrofuran; chloroform; water;
DOI:10.1016/S0040-4020(99)00050-2

Reference yield:

: 223394-03-4
[4-((E)-3-Naphthalen-1-yl-allyl)-piperidin-1-yl]-phenyl-methanone

: 223394-04-5
E-3--1-(naphth-1-yl)prop-1-ene

Guidance literature:: With diphenyldisulfane; In chloroform; for 240h; Yield given; Irradiation;
DOI:10.1016/S0040-4020(99)00050-2

Reference yield:

: 39171-65-8
bromo(naphthalen-1-ylmethyl)triphenyl-λ5-phosphane

: 223394-04-5
E-3--1-(naphth-1-yl)prop-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) nBuLi / 1.) THF, hexane, room temperature, 30 min, 2.) THF, -78 deg C -> room temperature, 2 h

2: PhSSPh / CHCl₃ / 240 h / Irradiation

With n-butyllithium; diphenyldisulfane; In chloroform;
DOI:10.1016/S0040-4020(99)00050-2