N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

Base Information

Chemical Name:N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide
CAS No.:1554475-48-7
Molecular Formula:C₂₃H₂₆N₄O₃
Molecular Weight:406.484
Hs Code.:

Synonyms:N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

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Chemical Property of N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

Chemical Property:

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Technology Process of N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

There total 6 articles about N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.8%

: 24019-66-7
3-allylsalicylaldehyde

: 380339-39-9
2-(4-benzoylpiperazin-1-yl)acetohydrazide

: 1554475-48-7
N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

Guidance literature:: With hydrogenchloride; In ethanol; Reflux;

Reference yield:

: 864442-44-4
ethyl 2-(4-benzoylpiperazin-1-yl)acetate

: 1554475-48-7
N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol; methanol / Reflux

2: hydrogenchloride / ethanol / Reflux

With hydrogenchloride; hydrazine; In methanol; ethanol;

Reference yield:

: 40004-08-8
1-(Ethoxycarbonylmethyl)piperazine

: 1554475-48-7
N′-[[2-hydroxy-3-(2-propenyl)phenyl]methylene]-4-benzoyl-1-piperazineacetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: hydrazine / ethanol; methanol / Reflux

3.1: hydrogenchloride / ethanol / Reflux

With hydrogenchloride; triethylamine; hydrazine; In tetrahydrofuran; methanol; ethanol;