methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

Base Information

Chemical Name:methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate
CAS No.:287120-03-0
Molecular Formula:C₁₆H₂₃NO₅
Molecular Weight:309.362
Hs Code.:

Synonyms:methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

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Chemical Property of methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

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Technology Process of methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

There total 4 articles about methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 287119-91-9
methyl 2-methoxy-5-(N-methylamino)phenylacetate

: 287120-03-0
methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

Guidance literature:: In tetrahydrofuran; Heating;
DOI:10.1039/b000135j

Reference yield:

: 138563-98-1
methyl 2-methoxy-5-nitrophenylacetate

: 287120-03-0
methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / ethanol / 3102.97 Torr

2: tetrahydrofuran / -20 °C

3: BH₃*DMS / tetrahydrofuran / 20 °C

4: 98 percent / tetrahydrofuran / Heating

With dimethylsulfide borane complex; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; 1: Reduction / 2: Formylation / 3: Reduction / 4: Acylation;
DOI:10.1039/b000135j

Reference yield:

: 138563-97-0
(5-amino-2-methoxy-phenyl)-acetic acid methyl ester

: 287120-03-0
methyl 2-methoxy-5-[N-methyl-N-(tert-butyloxycarbonyl)]aminophenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / -20 °C

2: BH₃*DMS / tetrahydrofuran / 20 °C

3: 98 percent / tetrahydrofuran / Heating

With dimethylsulfide borane complex; In tetrahydrofuran; 1: Formylation / 2: Reduction / 3: Acylation;
DOI:10.1039/b000135j