C₃₆H₄₅N₇O₅

Base Information

Chemical Name:C₃₆H₄₅N₇O₅
CAS No.:1312610-73-3
Molecular Formula:C₃₆H₄₅N₇O₅
Molecular Weight:655.797
Hs Code.:

C<sub>36</sub>H<sub>45</sub>N<sub>7</sub>O<sub>5</sub>

Synonyms:C₃₆H₄₅N₇O₅

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Chemical Property of C₃₆H₄₅N₇O₅

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Technology Process of C₃₆H₄₅N₇O₅

There total 11 articles about C₃₆H₄₅N₇O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1312610-72-2
C₃₆H₄₂ClN₇O₇

: 1312610-73-3
C₃₆H₄₅N₇O₅

Guidance literature:: With hydrogen; palladium(II) hydroxide; In methanol; at 50 ℃; for 24h; under 2585.81 Torr;

Reference yield:

: 126463-85-2
4-acetylamino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-73-3
C₃₆H₄₅N₇O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: sulfuric acid / methanol / 7 h / Reflux

2.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

6.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

6.2: -5 - 20 °C

7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

8.1: ammonium acetate / toluene / Reflux

9.1: boron tribromide / dichloromethane / -70 - 20 °C

9.2: Cooling with ice

9.3: 3 h / 20 °C / pH 7 - 8

10.1: hydrogen / palladium(II) hydroxide / methanol / 24 h / 50 °C / 2585.81 Torr

With tert.-butylnitrite; oxalyl dichloride; lithium hydroxide monohydrate; sulfuric acid; ammonium acetate; water; hydrogen; boron tribromide; sodium carbonate; N-ethyl-N,N-diisopropylamine; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium(II) hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 3.1: Suzuki Coupling;

Reference yield:

: 457947-61-4
4-amino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-73-3
C₃₆H₄₅N₇O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

5.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

5.2: -5 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

7.1: ammonium acetate / toluene / Reflux

8.1: boron tribromide / dichloromethane / -70 - 20 °C

8.2: Cooling with ice

8.3: 3 h / 20 °C / pH 7 - 8

9.1: hydrogen / palladium(II) hydroxide / methanol / 24 h / 50 °C / 2585.81 Torr

With tert.-butylnitrite; oxalyl dichloride; lithium hydroxide monohydrate; ammonium acetate; water; hydrogen; boron tribromide; sodium carbonate; N-ethyl-N,N-diisopropylamine; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium(II) hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 2.1: Suzuki Coupling;