bis(2-pyridylmethyl)-1,3-propanedithiol

Base Information

Chemical Name:bis(2-pyridylmethyl)-1,3-propanedithiol
CAS No.:221296-33-9
Molecular Formula:C₁₅H₁₈N₂S₂
Molecular Weight:290.453
Hs Code.:

Synonyms:bis(2-pyridylmethyl)-1,3-propanedithiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2-pyridylmethyl)-1,3-propanedithiol

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Technology Process of bis(2-pyridylmethyl)-1,3-propanedithiol

There total 1 articles about bis(2-pyridylmethyl)-1,3-propanedithiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-80-8
1.3-propanedithiol

: 4377-33-7
2-chloromethylpyridine

: 221296-33-9
bis(2-pyridylmethyl)-1,3-propanedithiol

Guidance literature:: With sodium ethanolate;
DOI:10.1016/j.poly.2011.08.025

Reference yield: 71.0%

: cobalt(II) chloride hexahydrate

: 221296-33-9
bis(2-pyridylmethyl)-1,3-propanedithiol

: 1161444-52-5,221295-96-1
[Co(1,3-bis(2-pyridylmethylthio)propane)Cl2]

Guidance literature:: In methanol; MeOH soln. of CoCl2 added dropwise to MeOH soln. of 1,3-bis(2-pyridylmethylthio)propane; stirred for 1 h; refluxed for 3 h; crystd. by slow evapn. at room temp.; filtered; washed with H2O and MeOH; dried in vac.; elem. anal.;
DOI:10.1016/j.poly.2009.02.039

Reference yield: 63.0%

: nickel(II) perchlorate hexahydrate

: 221296-33-9
bis(2-pyridylmethyl)-1,3-propanedithiol

: 143-66-8
sodium tetraphenyl borate

: C₁₉H₂₄N₄NiS₂⁽²⁺⁾*2C₂₄H₂₀B^(1-)

Guidance literature:: nickel(II) perchlorate hexahydrate; bis(2-pyridylmethyl)-1,3-propanedithiol; In methanol; at 20 ℃; for 24h; Inert atmosphere;

sodium tetraphenyl borate; In methanol;
DOI:10.1021/acs.inorgchem.8b00881