diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

Base Information

Chemical Name:diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate
CAS No.:132125-33-8
Molecular Formula:C₄₄H₄₈N₂O₇
Molecular Weight:716.874
Hs Code.:

Synonyms:diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

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Chemical Property of diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

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Technology Process of diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

There total 5 articles about diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87905-98-4
5-<(benzyloxycarbonyl)amino>pentanol

: 132125-33-8
diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / triethylamine (TEA) / CHCl₃ / 2 h / -20 °C

2: 1.) NaH, 2.) KI / 1.) DMSO, 2.) 5 d

With sodium hydride; triethylamine; potassium iodide; In chloroform;
DOI:10.1021/jm00108a004

Reference yield:

: 2508-29-4
5-hydroxypentylamine

: 132125-33-8
diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH / dioxane / 48 h / Ambient temperature

2: 93 percent / triethylamine (TEA) / CHCl₃ / 2 h / -20 °C

3: 1.) NaH, 2.) KI / 1.) DMSO, 2.) 5 d

With sodium hydroxide; sodium hydride; triethylamine; potassium iodide; In 1,4-dioxane; chloroform;
DOI:10.1021/jm00108a004

Reference yield:

: 13433-00-6
diethyl aminomalonate hydrochloride

: 132125-33-8
diethyl <<3-(1-naphthalenyl)-2-(1-naphthalenyl)-1-oxopropyl>amino>-2-<5-<<(phenylmethoxy)carbonyl>amino>pentyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 95.4 percent / triethylamine (TEA) / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, overnight

2: 1.) NaH, 2.) KI / 1.) DMSO, 2.) 5 d

With sodium hydride; triethylamine; potassium iodide; In dichloromethane;
DOI:10.1021/jm00108a004