3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

Base Information

Chemical Name:3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid
CAS No.:1335117-13-9
Molecular Formula:C₁₉H₁₄F₃NO₄S
Molecular Weight:409.386
Hs Code.:

Synonyms:3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

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Chemical Property of 3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

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Technology Process of 3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

There total 3 articles about 3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 20277-69-4
sodium methansulfinate

: 1586-30-7
6-bromo-3-methyl-2-(3-trifluoromethyl-phenyl)-quinoline-4-carboxylic acid

: 1335117-13-9
3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

Guidance literature:: With copper(l) iodide; In dimethyl sulfoxide; at 120 ℃; for 40h; Inert atmosphere;

Reference yield:

: 1533-03-5
3-(trifluoromethyl)propiophenone

: 1335117-13-9
3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol; water / 3 h / 85 °C

1.2: 0 °C / pH ~ 3

2.1: copper(l) iodide / dimethyl sulfoxide / 40 h / 120 °C / Inert atmosphere

With copper(l) iodide; potassium hydroxide; In ethanol; water; dimethyl sulfoxide;

Reference yield:

: 87-48-9
5-Bromo-1H-indole-2,3-dione

: 1335117-13-9
3-methyl-6-(methylsulfonyl)-2-[3-(trifluoromethyl)phenyl]-4-quinolinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol; water / 3 h / 85 °C

1.2: 0 °C / pH ~ 3

2.1: copper(l) iodide / dimethyl sulfoxide / 40 h / 120 °C / Inert atmosphere

With copper(l) iodide; potassium hydroxide; In ethanol; water; dimethyl sulfoxide;