1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

Base Information

Chemical Name:1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside
CAS No.:434948-95-5
Molecular Formula:C₃₄H₄₇NO₆
Molecular Weight:565.75
Hs Code.:

Synonyms:1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

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Chemical Property of 1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

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Technology Process of 1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

There total 1 articles about 1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 195006-97-4
dodecyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-β-D-allopyranoside

: 434948-95-5
1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1016/S0957-4166(01)00562-6

Reference yield: 81.0%

: 434948-95-5
1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

: 74-95-3
1,1-dibromomethane

: 434949-32-3
1-dodecyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-3-phenyl-2-propenoyl)-β-D-allopyranoside

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water; for 48h; Heating;
DOI:10.1016/S0957-4166(01)00562-6

Reference yield:

: 434948-95-5
1-dodecyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-3-phenyl-2-propenamido)-β-D-allopyranoside

: 98819-68-2
3-phenyl-(2R,3R)-oxiran-2-ylmethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / NaOH; tetrabutylammonium bromide / CH₂Cl₂; H₂O / 48 h / Heating

2: m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

3: sodium borohydride / tetrahydrofuran / 20 °C

With sodium hydroxide; sodium tetrahydroborate; tetrabutylammomium bromide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0957-4166(01)00562-6