Technology Process of C31H33NO16
There total 5 articles about C31H33NO16 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; hydrogen fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jm300348r
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1,1,4,7,10,10-hexamethyltriethylenetetramine; silver carbonate / acetonitrile / 0 - 20 °C / Inert atmosphere
2: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere
3: sodium methylate / tetrahydrofuran; methanol / 4 h / 0 °C / Inert atmosphere
4: allyl alcohol / 0.67 h / 20 °C / Inert atmosphere
5: pyridine / 72 h / 0 - 20 °C / Inert atmosphere
6: pyridine; hydrogen fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
pyridine; 1H-imidazole; 1,1,4,7,10,10-hexamethyltriethylenetetramine; hydrogen fluoride; sodium methylate; silver carbonate;
In
tetrahydrofuran; methanol; allyl alcohol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm300348r
- Guidance literature:
-
Multi-step reaction with 3 steps
1: allyl alcohol / 0.67 h / 20 °C / Inert atmosphere
2: pyridine / 72 h / 0 - 20 °C / Inert atmosphere
3: pyridine; hydrogen fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
pyridine; hydrogen fluoride;
In
tetrahydrofuran; allyl alcohol;
DOI:10.1021/jm300348r
