C₁₃H₁₈N₂O₂

Base Information

• Chemical Name: C₁₃H₁₈N₂O₂
• CAS No.: 1407163-92-1
• Molecular Formula: C₁₃H₁₈N₂O₂
• Molecular Weight: 234.298
• Mol file: 1407163-92-1.mol

Synonyms:C₁₃H₁₈N₂O₂

Chemical Property of C₁₃H₁₈N₂O₂

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₃H₁₈N₂O₂

There total 1 articles about C₁₃H₁₈N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

C13H20N2O (1407163-91-0) → C13H18N2O2 (1407163-92-1)

Guidance literature:

With tert.-butylhydroperoxide; manganese(III) triacetate dihydrate; In decane; ethyl acetate; at 18 ℃; for 16.5h; Molecular sieve;

DOI:10.1021/ol3026846

Reference yield: 73.0%

C13H18N2O2 (1407163-92-1) → C13H17IN2O2 (1407163-93-2)

Guidance literature:

With iodine; In pyridine; chloroform; at 18 ℃; for 16.2h; Inert atmosphere;

DOI:10.1021/ol3026846

Reference yield:

C13H18N2O2 (1407163-92-1) → C19H21N3O4 (1407163-94-3)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine / chloroform; pyridine / 16.2 h / 18 °C / Inert atmosphere

2: copper; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / dimethyl sulfoxide / 0.5 h / 70 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; iodine; copper; In pyridine; chloroform; dimethyl sulfoxide; 2: |Ullmann Condensation;

DOI:10.1021/ol3026846

upstream raw materials:

C₁₃H₂₀N₂O

Downstream raw materials:

C₁₉H₂₁N₃O₄

1-acetylaspidoalbidine

C₁₃H₁₇IN₂O₂