2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

Base Information

Chemical Name:2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide
CAS No.:133239-49-3
Molecular Formula:C₁₄H₁₄Cl₂N₄
Molecular Weight:309.198
Hs Code.:

Synonyms:2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

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Chemical Property of 2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

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Technology Process of 2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

There total 4 articles about 2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 133239-48-2
2-<(2,6-dichloro-3-methylphenyl)amino>benzenethioamide

: 133239-49-3
2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

Guidance literature:: With hydrazine hydrate; In methanol; for 5h; Ambient temperature;
DOI:10.1021/jm00065a002

Reference yield:

: 644-62-2
MECLOFENAMIC ACID

: 133239-49-3
2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: (COCl)2, DMF / CH₂Cl₂ / 1.) 0 deg C, 15 min, 2.) RT, 30 min

2: 29percent aq. NH₃ / CH₂Cl₂; tetrahydrofuran / 1 h / Ambient temperature

3: 57 percent / Lawesson's reagent / tetrahydrofuran / 1.) RT, 3 d, 2.) reflux, 2 h

4: 68 percent / NH₂NH₂*H₂O / methanol / 5 h / Ambient temperature

With Lawessons reagent; ammonium hydroxide; oxalyl dichloride; hydrazine hydrate; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00065a002

Reference yield:

: 22121-56-8
meclofenamic acid chloride

: 133239-49-3
2-<(2,6-dichloro-3-methylphenyl)amino>benzenecarboximidic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 29percent aq. NH₃ / CH₂Cl₂; tetrahydrofuran / 1 h / Ambient temperature

2: 57 percent / Lawesson's reagent / tetrahydrofuran / 1.) RT, 3 d, 2.) reflux, 2 h

3: 68 percent / NH₂NH₂*H₂O / methanol / 5 h / Ambient temperature

With Lawessons reagent; ammonium hydroxide; hydrazine hydrate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00065a002