2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

Base Information

Chemical Name:2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone
CAS No.:1190719-56-2
Molecular Formula:C₂₁H₂₁NO₂
Molecular Weight:319.403
Hs Code.:

Synonyms:2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

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Technology Process of 2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

There total 3 articles about 2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1190719-40-4
(E)-4-((1-methyl-1H-indol-2-yl)methoxy)-1-p-tolylbut-2-en-1-one

: 1190719-56-2
2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

Guidance literature:: With (S)-CPA; In toluene; at 0 ℃; for 0.166667h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200903462

Reference yield: 99.0%

: C₂₁H₂₁NO₂

: 1190719-56-2
2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

Guidance literature:: With C₄₉H₃₃F₃NO₅PS; In toluene; at -70 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0030-1260537

Reference yield: 93.0%

: 19832-78-1
1-(4-methylphenyl)prop-2-en-1-one

: 585571-70-6
2-(allyloxymethyl)-1-methyl-1H-indole

: 1190719-56-2
2-(9-methyl-1,3,4,9-tetrahydropyrano[3,4-b]indol-4-yl)-1-p-tolylethanone

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; (S)-CPA; In toluene; at 60 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200903462