1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

Base Information

Chemical Name:1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan
CAS No.:79613-12-0
Molecular Formula:C₁₄H₁₈ClNO₈S₂
Molecular Weight:427.884
Hs Code.:

Synonyms:1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

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Chemical Property of 1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

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Technology Process of 1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

There total 3 articles about 1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 79622-26-7
2-(4-Chloro-phenylcarbamoyl)-3,3-bis-methylsulfanyl-acrylic acid ethyl ester

: 79613-12-0
1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 70 ℃; for 4h;

Reference yield:

: 15386-84-2
ethyl 3-(4-chloroanilino)-3-oxopropionate

: 79613-12-0
1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylsulfoxide / 2 h / Ambient temperature

2: dimethylsulfoxide / 2 h / Ambient temperature

3: 58 percent / 30percent H₂O₂ / acetic acid / 4 h / 70 °C

With dihydrogen peroxide; sodium hydride; In acetic acid; dimethyl sulfoxide;

Reference yield:

: C₁₂H₁₀ClNO₃S₂^(2-)*2Na⁽¹⁺⁾

: 79613-12-0
1-Ethoxycarbonyl-1-(4-chlorphenyl-carbamoyl)-1-hydroxy-2,2-bis(methylsulfonyl)ethan

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfoxide / 2 h / Ambient temperature

2: 58 percent / 30percent H₂O₂ / acetic acid / 4 h / 70 °C

With dihydrogen peroxide; In acetic acid; dimethyl sulfoxide;