Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

Base Information

Chemical Name:Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester
CAS No.:193893-11-7
Molecular Formula:C₁₃H₂₀O₇S
Molecular Weight:320.364
Hs Code.:

Synonyms:Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

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Chemical Property of Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

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Technology Process of Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

There total 3 articles about Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 193893-10-6
Methanesulfonic acid (R)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-(4-methoxy-benzyloxy)-ethyl ester

: 193893-11-7
Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

Guidance literature:: With hydrogenchloride; In methanol; Ambient temperature;
DOI:10.1016/S0040-4020(97)00651-0

Reference yield:

: 193893-08-2
(R)-4-[(R)-1-Benzyloxy-2-(4-methoxy-benzyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolane

: 193893-11-7
Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / Raney Ni / ethanol / 1 h / 760 Torr / Ambient temperature

2: 98 percent / Et₃N / CH₂Cl₂ / 0 °C

3: 97 percent / aq. HCl / methanol / Ambient temperature

With hydrogenchloride; hydrogen; triethylamine; nickel; In methanol; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00651-0

Reference yield:

: 193893-09-3
(R)-1-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2-(4-methoxy-benzyloxy)-ethanol

: 193893-11-7
Methanesulfonic acid (1R,2R)-2,3-dihydroxy-1-(4-methoxy-benzyloxymethyl)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 0 °C

2: 97 percent / aq. HCl / methanol / Ambient temperature

With hydrogenchloride; triethylamine; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(97)00651-0