Technology Process of C38H46ClN3O8
There total 5 articles about C38H46ClN3O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H32ClNO9;
With
methanesulfonyl chloride; triethylamine;
In
N,N-dimethyl acetamide;
at -20 ℃;
for 0.5h;
Inert atmosphere;
4-aminomethylquinuclidine;
In
N,N-dimethyl acetamide;
at 0 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; selenium(IV) oxide / 24 h / 80 °C / Inert atmosphere
2.1: triethylamine / methanol / 1 h / 0 °C / Inert atmosphere
3.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 0.5 h / -20 °C / Inert atmosphere
3.2: 1 h / 0 °C / Inert atmosphere
With
pyridine; selenium(IV) oxide; methanesulfonyl chloride; triethylamine;
In
methanol; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / methanol / 1 h / 0 °C / Inert atmosphere
2.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 0.5 h / -20 °C / Inert atmosphere
2.2: 1 h / 0 °C / Inert atmosphere
With
methanesulfonyl chloride; triethylamine;
In
methanol; N,N-dimethyl acetamide;