N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine
CAS No.:1345700-42-6
Molecular Formula:C₃₃H₃₇N₇O₁₄
Molecular Weight:755.695
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

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Chemical Property of N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

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Technology Process of N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

There total 1 articles about N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345700-40-4
tert-butyl (1,3-diazido-2-(azidomethyl)propan-2-yl)carbamate

: 1345700-42-6
N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 8 h / 20 °C

2: triethylamine / methanol / 36 h / 20 °C / pH 9 / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; ethanol;
DOI:10.1055/s-0030-1260151

Reference yield: 95.0%

: 1345700-42-6
N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

: 1345700-43-7
1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1055/s-0030-1260151

Reference yield:

: 1345700-42-6
N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

: 1345700-44-8
3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; trifluoroacetic acid / dichloromethane / 8 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1055/s-0030-1260151