3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

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Chemical Name:3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide
CAS No.:1345700-44-8
Molecular Formula:C₅₃H₆₆N₁₆O₂₂
Molecular Weight:1279.2
Hs Code.:

Synonyms:3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

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Chemical Property of 3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

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Technology Process of 3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

There total 2 articles about 3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 350483-40-8
3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}benzoic acid

: 1345700-43-7
1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

: 1345700-44-8
3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

Guidance literature:: 3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0030-1260151

Reference yield:

: 1345700-42-6
N-(tert-butoxycarbonyl)-1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methylamine

: 1345700-44-8
3,4,5-tris{2-[2-(2-azidoethoxy)ethoxy]ethoxy}-N-{1,1,1-tris[(4-hydroxy-3-nitrophenyl)acetamidomethyl]methyl}benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; trifluoroacetic acid / dichloromethane / 8 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 24 h / 20 °C / Inert atmosphere

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1055/s-0030-1260151