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Technology Process of [(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO

[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO

Base Information
  • Chemical Name:[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO
  • CAS No.:105162-41-2
  • Molecular Formula:3C3H7NO*2C24H20B*C82H82P6Rh2S2
  • Molecular Weight:2381.09
  • Hs Code.:
[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)HRh(SH)]2<sup>(2+)</sup>*2B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>*3(CH<sub>3</sub>)2NCHO=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)HRh(SH)]2(B(C<sub>6</sub>H<sub>5</sub>)4)2*3(CH<sub>3</sub>)2NCHO

Synonyms:[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO

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Chemical Property of [(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO
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Technology Process of [(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO

There total 2 articles about [(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(triphos)RhCl(C<sub>2</sub>H<sub>4</sub>)
105139-41-1

(triphos)RhCl(C2H4)

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

N,N-dimethyl-formamide
68-12-2,33513-42-7

N,N-dimethyl-formamide

[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)HRh(SH)]2<sup>(2+)</sup>*2B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>*3(CH<sub>3</sub>)2NCHO=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)HRh(SH)]2(B(C<sub>6</sub>H<sub>5</sub>)4)2*3(CH<sub>3</sub>)2NCHO
105162-41-2

[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO

Guidance literature:
With H2S; In dichloromethane; N,N-dimethyl-formamide; treatment of Rh-complex with H2S (in CH2Cl2/DMF), addn. of NaBPh4 (in BuOH); crystn.;

Reference yield:

((triphos)Rh(μ-S)2Rh(triphos))(BPh4)2
105139-43-3

((triphos)Rh(μ-S)2Rh(triphos))(BPh4)2

[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)HRh(SH)]2<sup>(2+)</sup>*2B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>*3(CH<sub>3</sub>)2NCHO=[(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)HRh(SH)]2(B(C<sub>6</sub>H<sub>5</sub>)4)2*3(CH<sub>3</sub>)2NCHO
105162-41-2

[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(2+)*2B(C6H5)4(1-)*3(CH3)2NCHO=[(CH3C(CH2P(C6H5)2)3)HRh(SH)]2(B(C6H5)4)2*3(CH3)2NCHO

Guidance literature:
With H2; In not given; H2-stream, 4 h (quantitative formation);
upstream raw materials:

((triphos)Rh(μ-S)2Rh(triphos))(BPh4)2

(triphos)RhCl(C2H4)

sodium tetraphenyl borate

N,N-dimethyl-formamide

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