C₅₂H₆₄N₄S₂

Base Information

• Chemical Name: C₅₂H₆₄N₄S₂
• CAS No.: 1335290-15-7
• Molecular Formula: C₅₂H₆₄N₄S₂
• Molecular Weight: 809.239
• Mol file: 1335290-15-7.mol

Synonyms:C₅₂H₆₄N₄S₂

Chemical Property of C₅₂H₆₄N₄S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₂H₆₄N₄S₂

There total 6 articles about C₅₂H₆₄N₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C38H58N4S2 + benzil (134-81-6) → C52H64N4S2 (1335290-15-7)

Guidance literature:

With toluene-4-sulfonic acid; In chloroform; at 65 ℃; for 16h;

DOI:10.1021/ol202199v

Reference yield:

5,6-dinitro-4,7-di(thiophen-2-yl)benzo[c][1,2,5]thiadiazole (165190-73-8) → C52H64N4S2 (1335290-15-7)

Guidance literature:

Multi-step reaction with 4 steps

1: triethyl phosphite / 1,2-dichloro-benzene / 16 h / 180 °C / Inert atmosphere

2: potassium iodide; potassium hydroxide / dimethyl sulfoxide / 16 h / 80 °C

3: zinc / acetic acid / 0.25 h / 140 °C

4: toluene-4-sulfonic acid / chloroform / 16 h / 65 °C

With toluene-4-sulfonic acid; potassium iodide; potassium hydroxide; zinc; triethyl phosphite; In chloroform; acetic acid; dimethyl sulfoxide; 1,2-dichloro-benzene; 1: Cadogan annulation;

DOI:10.1021/ol202199v

Reference yield:

dithienopyrrolobenzothiadiazole (1335290-08-8) → C52H64N4S2 (1335290-15-7)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium iodide; potassium hydroxide / dimethyl sulfoxide / 16 h / 80 °C

2: zinc / acetic acid / 0.25 h / 140 °C

3: toluene-4-sulfonic acid / chloroform / 16 h / 65 °C

With toluene-4-sulfonic acid; potassium iodide; potassium hydroxide; zinc; In chloroform; acetic acid; dimethyl sulfoxide;

DOI:10.1021/ol202199v

upstream raw materials:

benzil

dithienopyrrolobenzothiadiazole

C₃₈H₅₄N₄S₃

4,7-dibromobenzo[c][1,2,5]thiadiazole