(4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

Base Information

Chemical Name:(4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one
CAS No.:128576-80-7
Molecular Formula:C₃₁H₂₆N₂O₃
Molecular Weight:474.559
Hs Code.:

Synonyms:(4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

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Technology Process of (4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

There total 1 articles about (4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 128576-75-0
1-methyl N-(9-phenylfluoren-9-yl)-3-benzylaspartate

: 128576-80-7
(4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

Guidance literature:: With diphenyl-phosphinic acid; triethylamine; In acetonitrile; at 50 ℃; for 12h;
DOI:10.1021/jo00304a011

Reference yield: 90.0%

: 128576-80-7
(4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

: 128576-81-8
(4R,5S)-4-benzyl-5-carboxy-1-(9-phenylfluoren-9-yl)-imidazolidin-2-one

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; for 72h;
DOI:10.1021/jo00304a011

Reference yield:

: 128576-80-7
(4R,5S)-4-benzyl-5-(methoxycarbonyl)-1-(9-phenylfluoren-9-yl)imidazolidin-2-one

: 128576-79-4
(4S,5R)-5-benzyl-4-(methoxycarbonyl)imidazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / aq. LiOH / tetrahydrofuran / 72 h

2: 96 percent / trifluoroacetic acid / CH₂Cl₂ / 25 °C

3: thionyl chloride / 12 h / Ambient temperature

With lithium hydroxide; thionyl chloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00304a011