2--4--L-2,4-diaminobutyric p-nitrophenyl ester

Base Information

Chemical Name:2--4--L-2,4-diaminobutyric p-nitrophenyl ester
CAS No.:125156-36-7
Molecular Formula:C₂₃H₂₇N₃O₈
Molecular Weight:473.483
Hs Code.:

2-<N-(benzoxycarbonyl)amino>-4-<N-(tert-butoxycarbonyl)amino>-L-2,4-diaminobutyric p-nitrophenyl ester

Synonyms:2--4--L-2,4-diaminobutyric p-nitrophenyl ester

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Chemical Property of 2--4--L-2,4-diaminobutyric p-nitrophenyl ester

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Technology Process of 2--4--L-2,4-diaminobutyric p-nitrophenyl ester

There total 4 articles about 2--4--L-2,4-diaminobutyric p-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 125156-36-7
2--4--L-2,4-diaminobutyric p-nitrophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / CuCO₃, Cu(OH)2, 1N aq. NaHCO₃ / dioxane

2: 90 percent / 1M aq. Na₂CO₃ / 1.5 h / 0 - 20 °C

3: DCC / ethyl acetate

With copper(II) carbonate; copper(II) hydroxide; sodium hydrogencarbonate; sodium carbonate; dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate;
DOI:10.1021/jm990111c

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 125156-36-7
2--4--L-2,4-diaminobutyric p-nitrophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1M aq. Na₂CO₃ / 1.5 h / 0 - 20 °C

2: DCC / ethyl acetate

With sodium carbonate; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1021/jm990111c

Reference yield:

: 10270-94-7
4--L-2,4-diaminobutyric acid

: 125156-36-7
2--4--L-2,4-diaminobutyric p-nitrophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1M aq. Na₂CO₃ / 1.5 h / 0 - 20 °C

2: DCC / ethyl acetate

With sodium carbonate; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1021/jm990111c